1-vinyl-4-dimethoxy-beta-carboline | CAS:26585-13-7

1-vinyl-4-dimethoxy-beta-carboline

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1-vinyl-4-dimethoxy-beta-carboline Description

Source:	The herbs of Picrasma javanica
Solvent:	Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Storage:	Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C). Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour. Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com
After receiving:	The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.

Structure Identification:

Molecules. 2014 Jun 25;19(7):8752-61.

Preparative separation of alkaloids from Picrasma quassioides (D. Don) Benn. by conventional and pH-zone-refining countercurrent chromatography.[Pubmed: 24968331 ]

METHODS AND RESULTS:
Two high-speed countercurrent chromatography (HSCCC) modes were compared by separation of major alkaloids from crude extract of Picrasma quassioides. The conventional HSCCC separation was performed with a two-phase solvent system composed of petroleum ether-ethyl acetate-methanol-water (5:5:4.5:5.5, v/v/v/v) with 200 mg loading. pH-Zone-refining CCC was performed with two-phase solvent system composed of petroleum ether-ethyl acetate-n-butanol-water (3:2:7:9, v/v/v/v) where triethylamine (10 mM) was added to the upper organic stationary phase and hydrochloric acid (5 mM) was added to the lower aqueous phase with 2 g loading. From 2 g of crude extract, 87 mg of 5-methoxycanthin-6-one (a), 38 mg of 1-methoxy-β-carboline (b), 134 mg of 1-ethyl-4,8-dimethoxy-β-carboline (c), 74 mg of 1-ethoxycarbonyl-β-carboline (d), 56 mg of 1-vinyl-4,8-dimethoxy-β-carboline (e) and 26 mg of 1-vinyl-4-dimethoxy-beta-carboline (f) were obtained with purities of over 97.0%.
CONCLUSIONS:
The results indicated that pH-zone-refining CCC is an excellent separations tool at the multigram level.

Product Name	1-vinyl-4-dimethoxy-beta-carboline
Price:
CAS No.:	26585-13-7
Catalog No.:	CFN92928
Molecular Formula:	C₁₄H₁₂N₂O
Molecular Weight:	224.26 g/mol
Purity:	>=98%
Type of Compound:	Alkaloids
Physical Desc.:	Powder
Source:	The herbs of Picrasma javanica
Solvent:	Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Download:	COA MSDS
Similar structural:	Comparison
Guestbook:

Size /Price /Stock	10 mM * 100 uL in DMSO / Inquiry / In-stock 10 mM * 1 mL in DMSO / Inquiry / In-stock
Related Libraries	Alkaloids Compound Library

	1 mg	5 mg	10 mg	20 mg	25 mg
1 mM	4.4591 mL	22.2955 mL	44.5911 mL	89.1822 mL	111.4777 mL
5 mM	0.8918 mL	4.4591 mL	8.9182 mL	17.8364 mL	22.2955 mL
10 mM	0.4459 mL	2.2296 mL	4.4591 mL	8.9182 mL	11.1478 mL
50 mM	0.0892 mL	0.4459 mL	0.8918 mL	1.7836 mL	2.2296 mL
100 mM	0.0446 mL	0.223 mL	0.4459 mL	0.8918 mL	1.1148 mL

CFN96545	Erythrinin G	1616592-61-0	354.35	C₂₀H₁₈O₆
CFN95549	Ganoderic acid GS-2	1206781-65-8	500.7	C₃₀H₄₄O₆
CFN98131	Rhynchophylline	76-66-4	384.47	C₂₂H₂₈N₂O₄
CFN89452	Carmichaenine A	2065228-59-1	541.67	C₃₁H₄₃NO₇