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8-Deacetylyunaconitine
8-Deacetylyunaconitine
ChemFaces products have been cited in many studies from excellent and top scientific journals
Product Name 8-Deacetylyunaconitine
Price:
CAS No.: 93460-55-0
Catalog No.: CFN89329
Molecular Formula: C33H47NO10
Molecular Weight: 617.73 g/mol
Purity: >=98%
Type of Compound: Alkaloids
Physical Desc.: Powder
Source: The roots of Aconitum Vilmorinian Radix.
Solvent: Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Download: COA    MSDS
Similar structural: Comparison (Web)  (SDF)
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10 mM * 1 mL in DMSO / Inquiry / In-stock
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Biological Activity
Description: 8-Deacetylyunaconitine is a natural product from Aconitum Vilmorinian Radix.
8-Deacetylyunaconitine Description
Source: The roots of Aconitum Vilmorinian Radix.
Solvent: Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Storage: Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C).

Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour.

Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com

After receiving: The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.
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Recently, ChemFaces products have been cited in many studies from excellent and top scientific journals

Cell. 2018 Jan 11;172(1-2):249-261.e12.
doi: 10.1016/j.cell.2017.12.019.
IF=36.216(2019)

PMID: 29328914

Cell Metab. 2020 Mar 3;31(3):534-548.e5.
doi: 10.1016/j.cmet.2020.01.002.
IF=22.415(2019)

PMID: 32004475

Mol Cell. 2017 Nov 16;68(4):673-685.e6.
doi: 10.1016/j.molcel.2017.10.022.
IF=14.548(2019)

PMID: 29149595

ACS Nano. 2018 Apr 24;12(4): 3385-3396.
doi: 10.1021/acsnano.7b08969.
IF=13.903(2019)

PMID: 29553709

Nature Plants. 2016 Dec 22;3: 16206.
doi: 10.1038/nplants.2016.205.
IF=13.297(2019)

PMID: 28005066

Sci Adv. 2018 Oct 24;4(10): eaat6994.
doi: 10.1126/sciadv.aat6994.
IF=12.804(2019)

PMID: 30417089
Calculate Dilution Ratios(Only for Reference)
1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 1.6188 mL 8.0942 mL 16.1883 mL 32.3766 mL 40.4708 mL
5 mM 0.3238 mL 1.6188 mL 3.2377 mL 6.4753 mL 8.0942 mL
10 mM 0.1619 mL 0.8094 mL 1.6188 mL 3.2377 mL 4.0471 mL
50 mM 0.0324 mL 0.1619 mL 0.3238 mL 0.6475 mL 0.8094 mL
100 mM 0.0162 mL 0.0809 mL 0.1619 mL 0.3238 mL 0.4047 mL
* Note: If you are in the process of experiment, it's need to make the dilution ratios of the samples. The dilution data of the sheet for your reference. Normally, it's can get a better solubility within lower of Concentrations.
Protocol
Structure Identification:
Zhong Yao Cai. 2015 May;38(5):988-91.
Chemical Constituents from Processed Products of Aconitum Vilmoriniani Radix.[Pubmed: 26767293]
To investigate the chemical constituents of the processed products of Aconitum Vilmorinian Radix.
METHODS AND RESULTS:
The constituents were isolated by repeated column chromatography over silica gel, alumina and RP-C18 as well as recrystallization. The structures were elucidated on the basis of spectral analysis and physicochemical properties. Ten compounds were obtained from the methanol extract, and they were identified as yunaconitine (1), 8-deacetyl-yunaconitine (2), geniculatine C (3), vilmorrianine B (4), vilmorrianine C(5), vilmorrianine D (6), talatisamine (7), β-sitosterol (8), β-daucosterol (9) and β-sitosterol acetate (10).
CONCLUSIONS:
All compounds are obtained from the processed products of Aconitum Vilmoriniani Radix for the first time.
J Sep Sci. 2013 Aug;36(16):2680-5.
Accelerated solvent extraction and pH-zone-refining counter-current chromatographic purification of yunaconitine and 8-deacetylyunaconitine from Aconitum vilmorinianum Kom.[Pubmed: 23784883]

METHODS AND RESULTS:
This study aimed to seek an efficient method to extract and purify yunaconitine and 8-Deacetylyunaconitine from Aconitum vilmorinianum Kom. by accelerated solvent extraction combined with pH-zone-refining counter-current chromatography. The major extraction parameters for accelerated solvent extraction were optimized by an orthogonal test design L9 (3)(4). Then a separation and purification method was established using pH-zone-refining counter-current chromatography with a two-phase solvent system composed of petroleum ether/ethyl acetate/methanol/water (5:5:2:8, v/v) with 10 mM triethylamine in the upper phase and 10 mM HCl in the lower phase. From 2 g crude extract, 224 mg of 8-Deacetylyunaconitine (I) and 841 mg of yunaconitine (II) were obtained with a purity of over 98.0%.
CONCLUSIONS:
The chemical structures were identified by ESI-MS and (1)H and (13)C NMR spectroscopy.
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