9-Methyl-9-azabicyclo[3.3.1]nonan-3-one | CAS:552-70-5

9-Methyl-9-azabicyclo[3.3.1]nonan-3-one

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9-Methyl-9-azabicyclo[3.3.1]nonan-3-one Description

Source:
Solvent:	Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Storage:	Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C). Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour. Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com
After receiving:	The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.

Structure Identification:

European Polymer Journal, 1996, 32(2):1877-1883.

11th Bratislava IUPAC International Conference on Polymers High Tatras. Thermal and photo-induced oxidation of polymers and its inhibition in the 21st century.[Reference: WebLink]

METHODS AND RESULTS:
The relative configurations of tert-butyldimethylsilyl (TBDMS) ethers of all four diastereomers of the aldols of tropinone (8-methyl-8-azabicyclo[3.2.1]octan-3-one), as well as of granatanone (9-Methyl-9-azabicyclo[3.3.1]nonan-3-one), were determined from NMR data, and from the observed interconversion of the diastereomers (exo,anti to endo,syn and exo,syn to endo,anti). The exo forms invert to endo isomers in the presence of silica gel.
CONCLUSIONS:
The relative configuration of a new isomer of tropinone aldol accessible synthetically through the direct solventless reaction of tropinone and benzaldehyde in the presence of water was determined as exo,syn by comparison of NMR data of the aldol isomers, in particular vicinal coupling constants and shifts corresponding to the side-chain CH group, with data of related TBDMS derivatives and confirmed by single-crystal X-ray diffraction.

Product Name	9-Methyl-9-azabicyclo[3.3.1]nonan-3-one
Price:	$30 / 20mg
CAS No.:	552-70-5
Catalog No.:	CFN70138
Molecular Formula:	C₉H₁₅NO
Molecular Weight:	153.2 g/mol
Purity:	>=98%
Type of Compound:	Alkaloids
Physical Desc.:	Powder
Source:
Solvent:	Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
Download:	COA MSDS
Similar structural:	Comparison
Guestbook:

Size /Price /Stock	10 mM * 100 uL in DMSO / Inquiry / In-stock 10 mM * 1 mL in DMSO / Inquiry / In-stock
Related Libraries	Alkaloids Compound Library

	1 mg	5 mg	10 mg	20 mg	25 mg
1 mM	6.5274 mL	32.6371 mL	65.2742 mL	130.5483 mL	163.1854 mL
5 mM	1.3055 mL	6.5274 mL	13.0548 mL	26.1097 mL	32.6371 mL
10 mM	0.6527 mL	3.2637 mL	6.5274 mL	13.0548 mL	16.3185 mL
50 mM	0.1305 mL	0.6527 mL	1.3055 mL	2.611 mL	3.2637 mL
100 mM	0.0653 mL	0.3264 mL	0.6527 mL	1.3055 mL	1.6319 mL

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